For the safe, precise and reliable elemental analysis of carbon (C) and sulfur (S) in predominantly organic matrices such as soils, waste, wood, oil, coal and coke, ELTRA offers the combustion analyzer ELEMENTRAC CS-r with IR detection.
The CS-r with up to 4 infrared cells is designed for carbon and sulfur measurement over a very wide concentration range. It uses a horizontal resistance furnace with ceramic tube, which operates in a range from 600 °C to 1550 °C.
The CS-r elemental analyzer meets or exceeds the requirements of all common ASTM, DIN, EN or ISO standards for elemental analysis.
The ELEMENTRAC CS-r analyzer determines the elements carbon and sulfur by combustion of the sample in an oxygen stream and subsequent measurement of the combustion gases CO2, SO2 and H2O in selective infrared measuring cells. A high sample weight of up to 500 mg ensures excellent reproducibility of the elemental analysis results, even for heterogeneous samples.
The high combustion temperatures and electronic monitoring of the oxygen flow allow complete oxidation of the sample and help to avoid too low results even with challenging materials like cement. Regardless of the selected configuration (carbon – sulfur - carbon and sulfur), operation is identical in all analyzer versions.
Volumes of 50 mg to 500 mg are typical for elemental analysis of carbon and sulfur. The sample is directly applied to a carrier (ceramic or Inconel boat) and analyzed without addition of accelerators.
The sample is placed in front of the furnace opening and the measurement is started in the software. Subsequently, the shutter opens, and the material can be introduced into the hot furnace. At the same time, the ELEMENTS software continuously records measured values during combustion. Closing the furnace during the measurement is optional and can improve reproducibility.
60 to 240 seconds after the analysis has started, the measured carbon and sulfur concentrations are available for export as a report or via LIMS. Depending on the selected configuration, carbon and sulfur values are available for the individual sample.
The ELEMENTRAC CS-r analyzer comes with various solutions for reliable and precise carbon and sulfur analysis.
For reliable carbon and sulfur analysis, the combustion gases must be freed from water vapor prior to IR detection. The CS-r elemental analyzer is equipped with two drying columns filled with magnesium perchlorate to reliably prevent absorption effects in large sample volumes. In the case of TOC analysis, a chemical tube can also be used as a halogen trap to reliably absorb acid residues and halogens.
The ELEMENTRAC CS-r and CHS-r analyzer series ensures safe and precise elemental analysis even of samples with low carbon content in the resistance furnace. Due to the optimized geometry of the sample port with reduced diameter, as well as an oxygen purge at the sample inlet, the CO2 blank value of the atmosphere during sample introduction is drastically reduced, thus enabling reliable carbon analysis in the low measuring range.
The CS-r elemental analyzer can be connected in any configuration to an additional furnace without detectors. This principle, known from the ELEMENTRAC CS-d, allows fast fractionated analysis by applying different temperatures and provides safety for high sample throughput.
Depending on the sample, carbon can also be present in the two different fractions TOC (Total Organic Carbon) or TIC (Total Inorganic Carbon). The CS-r elemental analyzer can be combined with ELTRA's TIC module to determine the TIC content via acidification. This combination enables reliable, direct TIC analysis in soils, building materials and other products in compliance with DIN EN 15936.
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The comprehensive Windows-based ELEMENTS software is an essential part of all ELEMENTRAC generation elemental analyzers.
A central window (analysis and results) is the starting point from which all functionalities required for the daily routine are easily accessible. From here it is possible to group and export analyzed samples, or register and analyze new ones. The user may call up various subordinate functionalities like application settings, calibration, diagnosis, or status.
biomass, building materials, coal / coke, fuels, oil, ores, plant materials, plastics, rubber, soil, soot, tobacco, waste, ...
coal
soil
plastic
| Measured elements | carbon, sulfur |
| Samples | organic |
| Furnace alignment | horizontal (resistance furnace) |
| Sample carrier | ceramic boats |
| Field of application | agriculture, biology, chemistry / plastics, coal / power plant, construction materials, environment / recycling, medicine / pharmaceuticals |
| Furnace | resistance furnace (ceramic tube), adjustable up to 1550 °C (steps of 1 °C) |
| Detection method | solid state infrared absorption |
| Number of IR cells | 1 - 4 |
| Material of IR path | gold |
| Typical analysis time | 60 - 180 s |
| Chemicals required | magnesium perchlorate, sodium hydroxide |
| Gas required | oxygen 99.5 % pure (2 - 4 bar / 30 - 60 psi) |
| Power requirements | 230 V, 50/60 H, max. heating up current 20 A |
| Dimensions (W x H x D) | 58 x 52 x 75 cm |
| Weight | ~ 77 kg |
| Required equipment | PC, monitor, balance (resolution 0.0001g) |
| Optional accessories | TIC module |
In the elemental analyzer CS-r the sample is burnt in an oxygen atmosphere at temperatures up to 1,550 °C. The furnace temperature can be freely selected in steps of 1 °C. The combustion gasses (CO2, H2O, SO2) coming from the furnace and pass through a dust filter. After the water vapor is chemically absorbed, the dried CO2 and SO2 gas is detected in the additional infrared cells. Depending on the configuration, it is possible to combine up to four (for C, S analyzers) infrared cells with different sensitivities.
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